Organic syntheses. V. 56
| Автор(ы): | Журнал
06.10.2007
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| Год изд.: | 1977 |
| Описание: | Пятьдесят шестой номер брошюры «Органический синтез» содержит описание следующих соединений: 5-ACETYL-1,2,3,4,5-PENTAMETHYLCYOLOPENTADIENE; ACYLAMIDOALKYL ACETOPHENONES FRОМ SUBSTITUTED PHENETHYLAMINES: 2-(2-ACETAMIDOETHYL)-4,5-DIMETHOXYACETOPHENONE; 3-ALKYLATED AND 3-ACYLATED INDOLES FROM A COMMON PRECURSOR: 3-BENZYLINDOLE AND 3-BENZOYLINDOLE; ortho-ALKYLATION OF ANILINES: ETHYL 4-AMINO-3-METHYLBENZOATE; ALKYLATION OF ISOQUINOLINE via 2-BENZOYL-1,2-DIHYDROISOQUINALDONITRILES: 1-BENZYLISOQUINOLINE; ALLYLIC OXIDATION WITH HYDROGEN PEROXIDE-SELENIUM DIOXIDE: trans-PINOCARVEOL; CARBOXYLATION OF AROMATIC COMPOUNDS: FERBOCENECARBOXYLIC ACID; CHAIN ELONGATION OP ALKENES via gem-DIHALOCYCLOPROPANES: 1,1-DIPHENYL-2-BROMO-3-ACETOXY-1-PROPENE; CONVERSION OF NITRO то CARBONYL BY OZONOLYSIS OF NITRONATES: 2,5-HEPTANEDIONE. А также некоторые другие. Всего рассмотрено 27 соединений. |
| Оглавление: |
Обложка книги.
ACYLAMIDOALKYL ACETOPHENONES FRОМ SUBSTITUTED PHENETHYLAMINES: 2-(2-ACETAMIDOETHYL)-4,5-DIMETHOXYACETOPHENONE [3] 3-ALKYLATED AND 3-ACYLATED INDOLES FROM A COMMON PRECURSOR: 3-BENZYLINDOLE AND 3-BENZOYLINDOLE [8] ortho-ALKYLATION OF ANILINES: ETHYL 4-AMINO-3-METHYLBENZOATE [15] ALKYLATION OF ISOQUINOLINE via 2-BENZOYL-1,2-DIHYDROISOQUINALDONITRILES: 1-BENZYLISOQUINOLINE [19] ALLYLIC OXIDATION WITH HYDROGEN PEROXIDE-SELENIUM DIOXIDE: trans-PINOCARVEOL [25] CARBOXYLATION OF AROMATIC COMPOUNDS: FERBOCENECARBOXYLIC ACID [28] CHAIN ELONGATION OP ALKENES via gem-DIHALOCYCLOPROPANES: 1,1-DIPHENYL-2-BROMO-3-ACETOXY-1-PROPENE [32] CONVERSION OF NITRO то CARBONYL BY OZONOLYSIS OF NITRONATES: 2,5-HEPTANEDIONE [36] CONVERSION OF PRIMARY ALCOHOLS TO URETHANES (?) THE INNER SALT OF METHYL (CARBOXYSULFAMOYL)TRIETHYLAMMONIUM HYDROXIDE: METHYL (?)-HEXYLCARBAMATE [40] DeMETHYLATION of METHYL ARYL ETHERS: 4-ETHOXY-3-HYDROXYBENZALDEHYDE [44] 5,6-DIHYDRO-2H-PYRAN-2-ONE AND 2H-PYRAN-2-ONE [49] ENONE EEDUCTION-ENOLATE ALKYLATION SEQUENCE: 2-ALLYL-3-METHYLCYCLOHEXANONE [52] ESTERIFICATION OF CARBOXYLIC ACIDS WITH TRIALKYLOXONIUM SALTS: ETHYL AND METHYL 4-ACETOXYBENZOATES [59] ETHYL (E)-3-NITROACRYLATE [65] FRЕЕ-RADICAL ALKYLATION OF QUINONES: 2-PHENOXYMETHYL-1,4-BENZOQUINONE [68] INDOLES FROM ANILINES: ETHYL 2-METHYLINDOLE-5-CARBOXYLATE [72] trans-IODOPROPENYLATION OF ALKYL, HALIDES: (E)-IODO-4-PHENYL-2-BUTENE [77] METHYL GROUPS BY REDUCTION OF AROMATIC CARBOXYLIC ACIDS WITH TRICHLOROSILANE-TRI-(?)-PROPYLAMINE: 2-METHYLBIPHENYL [83] PEPTIDE SYNTHESES USING N-ETHYL-5-PHENYLISOXAZOLIUM-3'-SULFONATE: CARBOBENZOXY-L-ASPARAGINYL-L-LEUCINE METHYL ESTER AND N-CARBOBENZOXY-3-HYDROXY-L-PBOLYLGLYCYLGLYCINE ETHYL ESTER [88] POLYMERIC CARBODIIMIDE. I. PREPARATION [95] POLYMERIC CARBODIIMIDE. II. MOFFAT OXIDATION: 4-tert-BUTYLCYCLO-HEXANONE [99] REDUCTIVE CLEAVAGE OF ALLYLIC ALCOHOLS, ETHERS, OR ACETATES TO OLEFINS: 3-METHYLCYCLOHEXENE [101] RING CONTRACTION via (?) FAVORSK(?-TYPE REARRANGEMENT: CYCLOUNDECANONE [107] SELECTIVE EPOXIDATION OF TERMINAL DOUBLE BONDS: 10,11-EPOXYFARNESYL ACETATE [112] 2,3,4,5-TETRAHYDHOPYRIDINE [118] TRIFLUOROACETYLATION OF AMINES AND AMINO ACIDS UNDER NEUTRAL, MILD CONDITIONS- N-TRIFLUOROACETANILIDE AND N-ТRIFLUOROACETYL-L-TYROSINE [122] AMINOACETONE SEMICARBAZONE HYDROCHLORIDE (CORRECTION) [127] IODOMETHANE (WARNING) [127] OSHA LIST OF CARCINOGENS (WARNING) [128] AUTHOR INDEX [129] SUBJECT INDEX [131] |
| Формат: | djvu |
| Размер: | 2293664 байт |
| Язык: | ENG |
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| Открыть: | Ссылка (RU) |